Your cart is empty.
  • Home

    200 and more NMR experiments : a practical course / Stefan Berger, Siegmar Braun.

    By: Berger, Stefan, 1946-Contributor(s): Braun, SiegmarMaterial type: TextTextPublisher: Weinheim : Wiley-VCH, c2004Edition: 3rd rev. and expanded edDescription: xv, 838 p. : ill. ; 24 cmISBN: 3527310673; 9783527310678Other title: Two hundred and more NMR experiments | NMR experimentsSubject(s): Nuclear magnetic resonance spectroscopyDDC classification: 543/.66 LOC classification: QD96.N8 | B47 2004Online resources: Publisher description | Table of contents only
    Contents:
    The NMR Spectrometer -- Components of an NMR Spectrometer -- The Magnet -- The Spectrometer Cabinet -- The Computer -- Maintenance -- Tuning a Probe-Head -- The Lock Channel -- The Art of Shimming -- The Shim Gradients -- The Shimming Procedure -- Gradient Shimming -- Determination of Pulse-Duration -- Determination of the 90[degree] [superscript 1]H Transmitter Pulse-Duration -- Determination of the 90[degree] [superscript 13]C Transmitter Pulse-Duration -- Determination of the 90[degree] [superscript 1]H Decoupler Pulse-Duration -- The 90[degree] [superscript 1]H Pulse with Inverse Spectrometer Configuration -- The 90[degree] [superscript 13]C Decoupler Pulse with Inverse Configuration -- Composite Pulses -- Radiation Damping -- Pulse and Receiver Phases -- Determination of Radiofrequency Power -- Routine NMR Spectroscopy and Standard Tests -- The Standard [superscript 1]H NMR Experiment -- The Standard [superscript 13]C NMR Experiment -- The Application of Window Functions -- Computer-Aided Spectral Analysis -- Line Shape Test for [superscript 1]H NMR Spectroscopy -- Resolution Test for [superscript 1]H NMR Spectroscopy -- Sensitivity Test for [superscript 1]H NMR Spectroscopy -- Line Shape Test for [superscript 13]C NMR Spectroscopy -- ASTM Sensitivity Test for [superscript 13]C NMR Spectroscopy -- Sensitivity Test for [superscript 13]C NMR Spectroscopy -- Quadrature Image Test -- Dynamic Range Test for Signal Amplitudes -- 13[degree] Phase Stability Test -- Radiofrequency Field Homogeneity -- Decoupling Techniques -- Decoupler Calibration for Homonuclear Decoupling -- Decoupler Calibration for Heteronuclear Decoupling -- Low-Power Calibration for Heteronuclear Decoupling -- Homonuclear Decoupling -- Homonuclear Decoupling at Two Frequencies -- The Homonuclear SPT Experiment -- The Heteronuclear SPT Experiment -- The Basic Homonuclear NOE Difference Experiment -- 1D Nuclear Overhauser Difference Spectroscopy -- 1D NOE Spectroscopy with Multiple Selective Irradiation -- [superscript 1]H Off-Resonance Decoupled [superscript 13]C NMR Spectra -- The Gated [superscript 1]H-Decoupling Technique -- The Inverse Gated [superscript 1]H-Decoupling Technique -- [superscript 1]H Single-Frequency Decoupling of [superscript 13]C NMR Spectra -- [superscript 1]H Low-Power Decoupling of [superscript 13]C NMR Spectra -- Measurement of the Heteronuclear Overhauser Effect -- Dynamic NMR Spectroscopy -- Low-Temperature Calibration Using Methanol -- High-Temperature Calibration Using 1,2-Ethanediol -- Dynamic [superscript 1]H NMR Spectroscopy on Dimethylformamide -- The Saturation Transfer Experiment -- Measurement of the Rotating-Frame Relaxation Time T[subscript 1 rho] -- 1D Multipulse Sequences -- Measurement of the Spin-Lattice Relaxation Time T[subscript 1] -- Measurement of the Spin-Spin Relaxation Time T[subscript 2] -- [superscript 13]C NMR Spectra with SEFT -- [superscript 13]C NMR Spectra with APT -- The Basic INEPT Technique -- INEPT+ -- Refocused INEPT -- Reverse INEPT -- DEPT-135 -- Editing [superscript 13]C NMR Spectra Using DEPT -- DEPTQ -- Multiplicity Determination Using PENDANT -- 1D-INADEQUATE -- The BIRD Filter -- TANGO -- The Heteronuclear Double-Quantum Filter -- Purging with a Spin-Lock Pulse -- Water Suppression by Presaturation -- Water Suppression by the Jump-and-Return Method -- NMR Spectroscopy with Selective Pulses -- Determination of a Shaped 90[degree] [superscript 1]H Transmitter Pulse -- Determination of a Shaped 90[degree] [superscript 1]H Decoupler Pulse -- Determination of a Shaped 90[degree] [superscript 13]C Decoupler Pulse -- Selective Excitation Using DANTE -- SELCOSY -- SELINCOR: Selective Inverse H,C Correlation via [superscript 1]J(C,H) -- SELINQUATE -- Selective TOCSY -- INAPT -- Determination of Long-Range C,H Coupling Constants -- SELRESOLV -- SERF -- Auxiliary Reagents, Quantitative Determinations, and Reaction Mechanisms -- Signal Separation Using a Lanthanide Shift Reagent -- Signal Separation of Enantiomers Using a Chiral Shift Reagent -- Signal Separation of Enantiomers Using a Chiral Solvating Agent -- Determination of Enantiomeric Purity with Pirkle's Reagent -- Determination of Enantiomeric Purity by [superscript 31]P NMR -- Determination of Absolute Configuration by the Advanced Mosher Method -- Aromatic Solvent-Induced Shift (ASIS) -- NMR Spectroscopy of OH Protons and H/D Exchange -- Water Suppression Using an Exchange Reagent -- Isotope Effects on Chemical Shielding -- pK[subscript a] Determination by [superscript 13]C NMR -- Determination of Association Constants K[subscript a] -- Saturation Transfer Difference NMR -- The Relaxation Reagent Cr(acac)[subscript 3] -- Determination of Paramagnetic Susceptibility by NMR -- [superscript 1]H and [superscript 13]C NMR of Paramagnetic Compounds -- The CIDNP Effect -- Quantitative [superscript 1]H NMR Spectroscopy: Determination of the Alcohol Content of Polish Vodka -- Quantitative [superscript 13]C NMR Spectroscopy with Inverse Gated [superscript 1]H-Decoupling -- NMR Using Liquid-Crystal Solvents -- Heteronuclear NMR Spectroscopy -- [superscript 1]H-Decoupled [superscript 15]N NMR Spectra Using DEPT -- [superscript 1]H-Coupled [superscript 15]N NMR Spectra Using DEPT -- [superscript 19]F NMR Spectroscopy -- [superscript 29]Si NMR Spectroscopy Using DEPT -- [superscript 29]Si NMR Spectroscopy Using Spin-Lock Polarization -- [superscript 119]Sn NMR Spectroscopy -- [superscript 2]H NMR Spectroscopy -- [superscript 11]B NMR Spectroscopy -- [superscript 17]O NMR Spectroscopy Using RIDE -- [superscript 47/49]Ti NMR Spectroscopy Using ARING -- The Second Dimension -- 2D J-Resolved [superscript 1]H NMR Spectroscopy -- 2D J-Resolved [superscript 13]C NMR Spectroscopy -- The Basic H,H-COSY Experiment -- Long-Range COSY -- Phase-Sensitive COSY -- Phase-Sensitive COSY-45 -- E.COSY -- Double-Quantum-Filtered COSY with Presaturation -- Fully Coupled C,H Correlation (FUCOUP) -- C,H-Correlation by Polarization Transfer (HETCOR) -- Long-Range C,H-Correlation by Polarization Transfer -- C,H Correlation via Long-Range Couplings (COLOC) -- The Basic HMQC Experiment -- Phase-Sensitive HMQC with BIRD Filter and GARP Decoupling -- Poor Man's Gradient HMQC -- Phase-Sensitive HMBC with BIRD Filter
    Tags from this library: No tags from this library for this title. Log in to add tags.
        Average rating: 0.0 (0 votes)
    Item type Current library Call number Copy number Status Notes Date due Barcode
    Books Books Main Library
    		QD96 .N8 B47 2004 (Browse shelf (Opens below)) 1 Available STACKS 51952000122388

    Includes bibliographical references and index.

    Chapter 1. The NMR Spectrometer -- 1.1. Components of an NMR Spectrometer -- 1.1.1. The Magnet -- 1.1.2. The Spectrometer Cabinet -- 1.1.3. The Computer -- 1.1.4. Maintenance -- 1.2. Tuning a Probe-Head -- 1.3. The Lock Channel -- 1.4. The Art of Shimming -- 1.4.1. The Shim Gradients -- 1.4.2. The Shimming Procedure -- 1.4.3. Gradient Shimming -- Chapter 2. Determination of Pulse-Duration -- Exp. 2.1. Determination of the 90[degree] [superscript 1]H Transmitter Pulse-Duration -- Exp. 2.2. Determination of the 90[degree] [superscript 13]C Transmitter Pulse-Duration -- Exp. 2.3. Determination of the 90[degree] [superscript 1]H Decoupler Pulse-Duration -- Exp. 2.4. The 90[degree] [superscript 1]H Pulse with Inverse Spectrometer Configuration -- Exp. 2.5. The 90[degree] [superscript 13]C Decoupler Pulse with Inverse Configuration -- Exp. 2.6. Composite Pulses -- Exp. 2.7. Radiation Damping -- Exp. 2.8. Pulse and Receiver Phases -- Exp. 2.9. Determination of Radiofrequency Power -- Chapter 3. Routine NMR Spectroscopy and Standard Tests -- Exp. 3.1. The Standard [superscript 1]H NMR Experiment -- Exp. 3.2. The Standard [superscript 13]C NMR Experiment -- Exp. 3.3. The Application of Window Functions -- Exp. 3.4. Computer-Aided Spectral Analysis -- Exp. 3.5. Line Shape Test for [superscript 1]H NMR Spectroscopy -- Exp. 3.6. Resolution Test for [superscript 1]H NMR Spectroscopy -- Exp. 3.7. Sensitivity Test for [superscript 1]H NMR Spectroscopy -- Exp. 3.8. Line Shape Test for [superscript 13]C NMR Spectroscopy -- Exp. 3.9. ASTM Sensitivity Test for [superscript 13]C NMR Spectroscopy -- Exp. 3.10. Sensitivity Test for [superscript 13]C NMR Spectroscopy -- Exp. 3.11. Quadrature Image Test -- Exp. 3.12. Dynamic Range Test for Signal Amplitudes -- Exp. 3.13. 13[degree] Phase Stability Test -- Exp. 3.14. Radiofrequency Field Homogeneity -- Chapter 4. Decoupling Techniques -- Exp. 4.1. Decoupler Calibration for Homonuclear Decoupling -- Exp. 4.2. Decoupler Calibration for Heteronuclear Decoupling -- Exp. 4.3. Low-Power Calibration for Heteronuclear Decoupling -- Exp. 4.4. Homonuclear Decoupling -- Exp. 4.5. Homonuclear Decoupling at Two Frequencies -- Exp. 4.6. The Homonuclear SPT Experiment -- Exp. 4.7. The Heteronuclear SPT Experiment -- Exp. 4.8. The Basic Homonuclear NOE Difference Experiment -- Exp. 4.9. 1D Nuclear Overhauser Difference Spectroscopy -- Exp. 4.10. 1D NOE Spectroscopy with Multiple Selective Irradiation -- Exp. 4.11. [superscript 1]H Off-Resonance Decoupled [superscript 13]C NMR Spectra -- Exp. 4.12. The Gated [superscript 1]H-Decoupling Technique -- Exp. 4.13. The Inverse Gated [superscript 1]H-Decoupling Technique -- Exp. 4.14. [superscript 1]H Single-Frequency Decoupling of [superscript 13]C NMR Spectra -- Exp. 4.15. [superscript 1]H Low-Power Decoupling of [superscript 13]C NMR Spectra -- Exp. 4.16. Measurement of the Heteronuclear Overhauser Effect -- Chapter 5. Dynamic NMR Spectroscopy -- Exp. 5.1. Low-Temperature Calibration Using Methanol -- Exp. 5.2. High-Temperature Calibration Using 1,2-Ethanediol -- Exp. 5.3. Dynamic [superscript 1]H NMR Spectroscopy on Dimethylformamide -- Exp. 5.4. The Saturation Transfer Experiment -- Exp. 5.5. Measurement of the Rotating-Frame Relaxation Time T[subscript 1 rho] -- Chapter 6. 1D Multipulse Sequences -- Exp. 6.1. Measurement of the Spin-Lattice Relaxation Time T[subscript 1] -- Exp. 6.2. Measurement of the Spin-Spin Relaxation Time T[subscript 2] -- Exp. 6.3. [superscript 13]C NMR Spectra with SEFT -- Exp. 6.4. [superscript 13]C NMR Spectra with APT -- Exp. 6.5. The Basic INEPT Technique -- Exp. 6.6. INEPT+ -- Exp. 6.7. Refocused INEPT -- Exp. 6.8. Reverse INEPT -- Exp. 6.9. DEPT-135 -- Exp. 6.10. Editing [superscript 13]C NMR Spectra Using DEPT -- Exp. 6.11. DEPTQ -- Exp. 6.12. Multiplicity Determination Using PENDANT -- Exp. 6.13. 1D-INADEQUATE -- Exp. 6.14. The BIRD Filter -- Exp. 6.15. TANGO -- Exp. 6.16. The Heteronuclear Double-Quantum Filter -- Exp. 6.17. Purging with a Spin-Lock Pulse -- Exp. 6.18. Water Suppression by Presaturation -- Exp. 6.19. Water Suppression by the Jump-and-Return Method -- Chapter 7. NMR Spectroscopy with Selective Pulses -- Exp. 7.1. Determination of a Shaped 90[degree] [superscript 1]H Transmitter Pulse -- Exp. 7.2. Determination of a Shaped 90[degree] [superscript 1]H Decoupler Pulse -- Exp. 7.3. Determination of a Shaped 90[degree] [superscript 13]C Decoupler Pulse -- Exp. 7.4. Selective Excitation Using DANTE -- Exp. 7.5. SELCOSY -- Exp. 7.6. SELINCOR: Selective Inverse H,C Correlation via [superscript 1]J(C,H) -- Exp. 7.7. SELINQUATE -- Exp. 7.8. Selective TOCSY -- Exp. 7.9. INAPT -- Exp. 7.10. Determination of Long-Range C,H Coupling Constants -- Exp. 7.11. SELRESOLV -- Exp. 7.12. SERF -- Chapter 8. Auxiliary Reagents, Quantitative Determinations, and Reaction Mechanisms -- Exp. 8.1. Signal Separation Using a Lanthanide Shift Reagent -- Exp. 8.2. Signal Separation of Enantiomers Using a Chiral Shift Reagent -- Exp. 8.3. Signal Separation of Enantiomers Using a Chiral Solvating Agent -- Exp. 8.4. Determination of Enantiomeric Purity with Pirkle's Reagent -- Exp. 8.5. Determination of Enantiomeric Purity by [superscript 31]P NMR -- Exp. 8.6. Determination of Absolute Configuration by the Advanced Mosher Method -- Exp. 8.7. Aromatic Solvent-Induced Shift (ASIS) -- Exp. 8.8. NMR Spectroscopy of OH Protons and H/D Exchange -- Exp. 8.9. Water Suppression Using an Exchange Reagent -- Exp. 8.10. Isotope Effects on Chemical Shielding -- Exp. 8.11. pK[subscript a] Determination by [superscript 13]C NMR -- Exp. 8.12. Determination of Association Constants K[subscript a] -- Exp. 8.13. Saturation Transfer Difference NMR -- Exp. 8.14. The Relaxation Reagent Cr(acac)[subscript 3] -- Exp. 8.15. Determination of Paramagnetic Susceptibility by NMR -- Exp. 8.16. [superscript 1]H and [superscript 13]C NMR of Paramagnetic Compounds -- Exp. 8.17. The CIDNP Effect -- Exp. 8.18. Quantitative [superscript 1]H NMR Spectroscopy: Determination of the Alcohol Content of Polish Vodka -- Exp. 8.19. Quantitative [superscript 13]C NMR Spectroscopy with Inverse Gated [superscript 1]H-Decoupling -- Exp. 8.20. NMR Using Liquid-Crystal Solvents -- Chapter 9. Heteronuclear NMR Spectroscopy -- Exp. 9.1. [superscript 1]H-Decoupled [superscript 15]N NMR Spectra Using DEPT -- Exp. 9.2. [superscript 1]H-Coupled [superscript 15]N NMR Spectra Using DEPT -- Exp. 9.3. [superscript 19]F NMR Spectroscopy -- Exp. 9.4. [superscript 29]Si NMR Spectroscopy Using DEPT -- Exp. 9.5. [superscript 29]Si NMR Spectroscopy Using Spin-Lock Polarization -- Exp. 9.6. [superscript 119]Sn NMR Spectroscopy -- Exp. 9.7. [superscript 2]H NMR Spectroscopy -- Exp. 9.8. [superscript 11]B NMR Spectroscopy -- Exp. 9.9. [superscript 17]O NMR Spectroscopy Using RIDE -- Exp. 9.10. [superscript 47/49]Ti NMR Spectroscopy Using ARING -- Chapter 10. The Second Dimension -- Exp. 10.1. 2D J-Resolved [superscript 1]H NMR Spectroscopy -- Exp. 10.2. 2D J-Resolved [superscript 13]C NMR Spectroscopy -- Exp. 10.3. The Basic H,H-COSY Experiment -- Exp. 10.4. Long-Range COSY -- Exp. 10.5. Phase-Sensitive COSY -- Exp. 10.6. Phase-Sensitive COSY-45 -- Exp. 10.7. E.COSY -- Exp. 10.8. Double-Quantum-Filtered COSY with Presaturation -- Exp. 10.9. Fully Coupled C,H Correlation (FUCOUP) -- Exp. 10.10. C,H-Correlation by Polarization Transfer (HETCOR) -- Exp. 10.11. Long-Range C,H-Correlation by Polarization Transfer -- Exp. 10.12. C,H Correlation via Long-Range Couplings (COLOC) -- Exp. 10.13. The Basic HMQC Experiment -- Exp. 10.14. Phase-Sensitive HMQC with BIRD Filter and GARP Decoupling -- Exp. 10.15. Poor Man's Gradient HMQC -- Exp. 10.16. Phase-Sensitive HMBC with BIRD Filter

    1

    There are no comments on this title.

    to post a comment.