200 and more NMR experiments : a practical course /
Two hundred and more NMR experiments NMR experiments
Stefan Berger, Siegmar Braun.
- 3rd rev. and expanded ed.
- Weinheim : Wiley-VCH, c2004.
- xv, 838 p. : ill. ; 24 cm.
Includes bibliographical references and index.
The NMR Spectrometer -- Components of an NMR Spectrometer -- The Magnet -- The Spectrometer Cabinet -- The Computer -- Maintenance -- Tuning a Probe-Head -- The Lock Channel -- The Art of Shimming -- The Shim Gradients -- The Shimming Procedure -- Gradient Shimming -- Determination of Pulse-Duration -- Determination of the 90[degree] [superscript 1]H Transmitter Pulse-Duration -- Determination of the 90[degree] [superscript 13]C Transmitter Pulse-Duration -- Determination of the 90[degree] [superscript 1]H Decoupler Pulse-Duration -- The 90[degree] [superscript 1]H Pulse with Inverse Spectrometer Configuration -- The 90[degree] [superscript 13]C Decoupler Pulse with Inverse Configuration -- Composite Pulses -- Radiation Damping -- Pulse and Receiver Phases -- Determination of Radiofrequency Power -- Routine NMR Spectroscopy and Standard Tests -- The Standard [superscript 1]H NMR Experiment -- The Standard [superscript 13]C NMR Experiment -- The Application of Window Functions -- Computer-Aided Spectral Analysis -- Line Shape Test for [superscript 1]H NMR Spectroscopy -- Resolution Test for [superscript 1]H NMR Spectroscopy -- Sensitivity Test for [superscript 1]H NMR Spectroscopy -- Line Shape Test for [superscript 13]C NMR Spectroscopy -- ASTM Sensitivity Test for [superscript 13]C NMR Spectroscopy -- Sensitivity Test for [superscript 13]C NMR Spectroscopy -- Quadrature Image Test -- Dynamic Range Test for Signal Amplitudes -- 13[degree] Phase Stability Test -- Radiofrequency Field Homogeneity -- Decoupling Techniques -- Decoupler Calibration for Homonuclear Decoupling -- Decoupler Calibration for Heteronuclear Decoupling -- Low-Power Calibration for Heteronuclear Decoupling -- Homonuclear Decoupling -- Homonuclear Decoupling at Two Frequencies -- The Homonuclear SPT Experiment -- The Heteronuclear SPT Experiment -- The Basic Homonuclear NOE Difference Experiment -- 1D Nuclear Overhauser Difference Spectroscopy -- 1D NOE Spectroscopy with Multiple Selective Irradiation -- [superscript 1]H Off-Resonance Decoupled [superscript 13]C NMR Spectra -- The Gated [superscript 1]H-Decoupling Technique -- The Inverse Gated [superscript 1]H-Decoupling Technique -- [superscript 1]H Single-Frequency Decoupling of [superscript 13]C NMR Spectra -- [superscript 1]H Low-Power Decoupling of [superscript 13]C NMR Spectra -- Measurement of the Heteronuclear Overhauser Effect -- Dynamic NMR Spectroscopy -- Low-Temperature Calibration Using Methanol -- High-Temperature Calibration Using 1,2-Ethanediol -- Dynamic [superscript 1]H NMR Spectroscopy on Dimethylformamide -- The Saturation Transfer Experiment -- Measurement of the Rotating-Frame Relaxation Time T[subscript 1 rho] -- 1D Multipulse Sequences -- Measurement of the Spin-Lattice Relaxation Time T[subscript 1] -- Measurement of the Spin-Spin Relaxation Time T[subscript 2] -- [superscript 13]C NMR Spectra with SEFT -- [superscript 13]C NMR Spectra with APT -- The Basic INEPT Technique -- INEPT+ -- Refocused INEPT -- Reverse INEPT -- DEPT-135 -- Editing [superscript 13]C NMR Spectra Using DEPT -- DEPTQ -- Multiplicity Determination Using PENDANT -- 1D-INADEQUATE -- The BIRD Filter -- TANGO -- The Heteronuclear Double-Quantum Filter -- Purging with a Spin-Lock Pulse -- Water Suppression by Presaturation -- Water Suppression by the Jump-and-Return Method -- NMR Spectroscopy with Selective Pulses -- Determination of a Shaped 90[degree] [superscript 1]H Transmitter Pulse -- Determination of a Shaped 90[degree] [superscript 1]H Decoupler Pulse -- Determination of a Shaped 90[degree] [superscript 13]C Decoupler Pulse -- Selective Excitation Using DANTE -- SELCOSY -- SELINCOR: Selective Inverse H,C Correlation via [superscript 1]J(C,H) -- SELINQUATE -- Selective TOCSY -- INAPT -- Determination of Long-Range C,H Coupling Constants -- SELRESOLV -- SERF -- Auxiliary Reagents, Quantitative Determinations, and Reaction Mechanisms -- Signal Separation Using a Lanthanide Shift Reagent -- Signal Separation of Enantiomers Using a Chiral Shift Reagent -- Signal Separation of Enantiomers Using a Chiral Solvating Agent -- Determination of Enantiomeric Purity with Pirkle's Reagent -- Determination of Enantiomeric Purity by [superscript 31]P NMR -- Determination of Absolute Configuration by the Advanced Mosher Method -- Aromatic Solvent-Induced Shift (ASIS) -- NMR Spectroscopy of OH Protons and H/D Exchange -- Water Suppression Using an Exchange Reagent -- Isotope Effects on Chemical Shielding -- pK[subscript a] Determination by [superscript 13]C NMR -- Determination of Association Constants K[subscript a] -- Saturation Transfer Difference NMR -- The Relaxation Reagent Cr(acac)[subscript 3] -- Determination of Paramagnetic Susceptibility by NMR -- [superscript 1]H and [superscript 13]C NMR of Paramagnetic Compounds -- The CIDNP Effect -- Quantitative [superscript 1]H NMR Spectroscopy: Determination of the Alcohol Content of Polish Vodka -- Quantitative [superscript 13]C NMR Spectroscopy with Inverse Gated [superscript 1]H-Decoupling -- NMR Using Liquid-Crystal Solvents -- Heteronuclear NMR Spectroscopy -- [superscript 1]H-Decoupled [superscript 15]N NMR Spectra Using DEPT -- [superscript 1]H-Coupled [superscript 15]N NMR Spectra Using DEPT -- [superscript 19]F NMR Spectroscopy -- [superscript 29]Si NMR Spectroscopy Using DEPT -- [superscript 29]Si NMR Spectroscopy Using Spin-Lock Polarization -- [superscript 119]Sn NMR Spectroscopy -- [superscript 2]H NMR Spectroscopy -- [superscript 11]B NMR Spectroscopy -- [superscript 17]O NMR Spectroscopy Using RIDE -- [superscript 47/49]Ti NMR Spectroscopy Using ARING -- The Second Dimension -- 2D J-Resolved [superscript 1]H NMR Spectroscopy -- 2D J-Resolved [superscript 13]C NMR Spectroscopy -- The Basic H,H-COSY Experiment -- Long-Range COSY -- Phase-Sensitive COSY -- Phase-Sensitive COSY-45 -- E.COSY -- Double-Quantum-Filtered COSY with Presaturation -- Fully Coupled C,H Correlation (FUCOUP) -- C,H-Correlation by Polarization Transfer (HETCOR) -- Long-Range C,H-Correlation by Polarization Transfer -- C,H Correlation via Long-Range Couplings (COLOC) -- The Basic HMQC Experiment -- Phase-Sensitive HMQC with BIRD Filter and GARP Decoupling -- Poor Man's Gradient HMQC -- Phase-Sensitive HMBC with BIRD Filter Chapter 1. 1.1. 1.1.1. 1.1.2. 1.1.3. 1.1.4. 1.2. 1.3. 1.4. 1.4.1. 1.4.2. 1.4.3. Chapter 2. Exp. 2.1. Exp. 2.2. Exp. 2.3. Exp. 2.4. Exp. 2.5. Exp. 2.6. Exp. 2.7. Exp. 2.8. Exp. 2.9. Chapter 3. Exp. 3.1. Exp. 3.2. Exp. 3.3. Exp. 3.4. Exp. 3.5. Exp. 3.6. Exp. 3.7. Exp. 3.8. Exp. 3.9. Exp. 3.10. Exp. 3.11. Exp. 3.12. Exp. 3.13. Exp. 3.14. Chapter 4. Exp. 4.1. Exp. 4.2. Exp. 4.3. Exp. 4.4. Exp. 4.5. Exp. 4.6. Exp. 4.7. Exp. 4.8. Exp. 4.9. Exp. 4.10. Exp. 4.11. Exp. 4.12. Exp. 4.13. Exp. 4.14. Exp. 4.15. Exp. 4.16. Chapter 5. Exp. 5.1. Exp. 5.2. Exp. 5.3. Exp. 5.4. Exp. 5.5. Chapter 6. Exp. 6.1. Exp. 6.2. Exp. 6.3. Exp. 6.4. Exp. 6.5. Exp. 6.6. Exp. 6.7. Exp. 6.8. Exp. 6.9. Exp. 6.10. Exp. 6.11. Exp. 6.12. Exp. 6.13. Exp. 6.14. Exp. 6.15. Exp. 6.16. Exp. 6.17. Exp. 6.18. Exp. 6.19. Chapter 7. Exp. 7.1. Exp. 7.2. Exp. 7.3. Exp. 7.4. Exp. 7.5. Exp. 7.6. Exp. 7.7. Exp. 7.8. Exp. 7.9. Exp. 7.10. Exp. 7.11. Exp. 7.12. Chapter 8. Exp. 8.1. Exp. 8.2. Exp. 8.3. Exp. 8.4. Exp. 8.5. Exp. 8.6. Exp. 8.7. Exp. 8.8. Exp. 8.9. Exp. 8.10. Exp. 8.11. Exp. 8.12. Exp. 8.13. Exp. 8.14. Exp. 8.15. Exp. 8.16. Exp. 8.17. Exp. 8.18. Exp. 8.19. Exp. 8.20. Chapter 9. Exp. 9.1. Exp. 9.2. Exp. 9.3. Exp. 9.4. Exp. 9.5. Exp. 9.6. Exp. 9.7. Exp. 9.8. Exp. 9.9. Exp. 9.10. Chapter 10. Exp. 10.1. Exp. 10.2. Exp. 10.3. Exp. 10.4. Exp. 10.5. Exp. 10.6. Exp. 10.7. Exp. 10.8. Exp. 10.9. Exp. 10.10. Exp. 10.11. Exp. 10.12. Exp. 10.13. Exp. 10.14. Exp. 10.15. Exp. 10.16.