TY  - BOOK
AU  - Berger,Stefan
AU  - Braun,Siegmar
TI  - 200 and more NMR experiments: a practical course 
SN  - 3527310673
AV  - QD96.N8 B47 2004
U1  - 543/.66 22
PY  - 2004///
CY  - Weinheim
PB  - Wiley-VCH
KW  - Nuclear magnetic resonance spectroscopy
N1  - Includes bibliographical references and index; Chapter 1; The NMR Spectrometer --; 1.1; Components of an NMR Spectrometer --; 1.1.1; The Magnet --; 1.1.2; The Spectrometer Cabinet --; 1.1.3; The Computer --; 1.1.4; Maintenance --; 1.2; Tuning a Probe-Head --; 1.3; The Lock Channel --; 1.4; The Art of Shimming --; 1.4.1; The Shim Gradients --; 1.4.2; The Shimming Procedure --; 1.4.3; Gradient Shimming --; Chapter 2; Determination of Pulse-Duration --; Exp. 2.1; Determination of the 90[degree] [superscript 1]H Transmitter Pulse-Duration --; Exp. 2.2; Determination of the 90[degree] [superscript 13]C Transmitter Pulse-Duration --; Exp. 2.3; Determination of the 90[degree] [superscript 1]H Decoupler Pulse-Duration --; Exp. 2.4; The 90[degree] [superscript 1]H Pulse with Inverse Spectrometer Configuration --; Exp. 2.5; The 90[degree] [superscript 13]C Decoupler Pulse with Inverse Configuration --; Exp. 2.6; Composite Pulses --; Exp. 2.7; Radiation Damping --; Exp. 2.8; Pulse and Receiver Phases --; Exp. 2.9; Determination of Radiofrequency Power --; Chapter 3; Routine NMR Spectroscopy and Standard Tests --; Exp. 3.1; The Standard [superscript 1]H NMR Experiment --; Exp. 3.2; The Standard [superscript 13]C NMR Experiment --; Exp. 3.3; The Application of Window Functions --; Exp. 3.4; Computer-Aided Spectral Analysis --; Exp. 3.5; Line Shape Test for [superscript 1]H NMR Spectroscopy --; Exp. 3.6; Resolution Test for [superscript 1]H NMR Spectroscopy --; Exp. 3.7; Sensitivity Test for [superscript 1]H NMR Spectroscopy --; Exp. 3.8; Line Shape Test for [superscript 13]C NMR Spectroscopy --; Exp. 3.9; ASTM Sensitivity Test for [superscript 13]C NMR Spectroscopy --; Exp. 3.10; Sensitivity Test for [superscript 13]C NMR Spectroscopy --; Exp. 3.11; Quadrature Image Test --; Exp. 3.12; Dynamic Range Test for Signal Amplitudes --; Exp. 3.13; 13[degree] Phase Stability Test --; Exp. 3.14; Radiofrequency Field Homogeneity --; Chapter 4; Decoupling Techniques --; Exp. 4.1; Decoupler Calibration for Homonuclear Decoupling --; Exp. 4.2; Decoupler Calibration for Heteronuclear Decoupling --; Exp. 4.3; Low-Power Calibration for Heteronuclear Decoupling --; Exp. 4.4; Homonuclear Decoupling --; Exp. 4.5; Homonuclear Decoupling at Two Frequencies --; Exp. 4.6; The Homonuclear SPT Experiment --; Exp. 4.7; The Heteronuclear SPT Experiment --; Exp. 4.8; The Basic Homonuclear NOE Difference Experiment --; Exp. 4.9; 1D Nuclear Overhauser Difference Spectroscopy --; Exp. 4.10; 1D NOE Spectroscopy with Multiple Selective Irradiation --; Exp. 4.11; [superscript 1]H Off-Resonance Decoupled [superscript 13]C NMR Spectra --; Exp. 4.12; The Gated [superscript 1]H-Decoupling Technique --; Exp. 4.13; The Inverse Gated [superscript 1]H-Decoupling Technique --; Exp. 4.14; [superscript 1]H Single-Frequency Decoupling of [superscript 13]C NMR Spectra --; Exp. 4.15; [superscript 1]H Low-Power Decoupling of [superscript 13]C NMR Spectra --; Exp. 4.16; Measurement of the Heteronuclear Overhauser Effect --; Chapter 5; Dynamic NMR Spectroscopy --; Exp. 5.1; Low-Temperature Calibration Using Methanol --; Exp. 5.2; High-Temperature Calibration Using 1,2-Ethanediol --; Exp. 5.3; Dynamic [superscript 1]H NMR Spectroscopy on Dimethylformamide --; Exp. 5.4; The Saturation Transfer Experiment --; Exp. 5.5; Measurement of the Rotating-Frame Relaxation Time T[subscript 1 rho] --; Chapter 6; 1D Multipulse Sequences --; Exp. 6.1; Measurement of the Spin-Lattice Relaxation Time T[subscript 1] --; Exp. 6.2; Measurement of the Spin-Spin Relaxation Time T[subscript 2] --; Exp. 6.3; [superscript 13]C NMR Spectra with SEFT --; Exp. 6.4; [superscript 13]C NMR Spectra with APT --; Exp. 6.5; The Basic INEPT Technique --; Exp. 6.6; INEPT+ --; Exp. 6.7; Refocused INEPT --; Exp. 6.8; Reverse INEPT --; Exp. 6.9; DEPT-135 --; Exp. 6.10; Editing [superscript 13]C NMR Spectra Using DEPT --; Exp. 6.11; DEPTQ --; Exp. 6.12; Multiplicity Determination Using PENDANT --; Exp. 6.13; 1D-INADEQUATE --; Exp. 6.14; The BIRD Filter --; Exp. 6.15; TANGO --; Exp. 6.16; The Heteronuclear Double-Quantum Filter --; Exp. 6.17; Purging with a Spin-Lock Pulse --; Exp. 6.18; Water Suppression by Presaturation --; Exp. 6.19; Water Suppression by the Jump-and-Return Method --; Chapter 7; NMR Spectroscopy with Selective Pulses --; Exp. 7.1; Determination of a Shaped 90[degree] [superscript 1]H Transmitter Pulse --; Exp. 7.2; Determination of a Shaped 90[degree] [superscript 1]H Decoupler Pulse --; Exp. 7.3; Determination of a Shaped 90[degree] [superscript 13]C Decoupler Pulse --; Exp. 7.4; Selective Excitation Using DANTE --; Exp. 7.5; SELCOSY --; Exp. 7.6; SELINCOR: Selective Inverse H,C Correlation via [superscript 1]J(C,H) --; Exp. 7.7; SELINQUATE --; Exp. 7.8; Selective TOCSY --; Exp. 7.9; INAPT --; Exp. 7.10; Determination of Long-Range C,H Coupling Constants --; Exp. 7.11; SELRESOLV --; Exp. 7.12; SERF --; Chapter 8; Auxiliary Reagents, Quantitative Determinations, and Reaction Mechanisms --; Exp. 8.1; Signal Separation Using a Lanthanide Shift Reagent --; Exp. 8.2; Signal Separation of Enantiomers Using a Chiral Shift Reagent --; Exp. 8.3; Signal Separation of Enantiomers Using a Chiral Solvating Agent --; Exp. 8.4; Determination of Enantiomeric Purity with Pirkle's Reagent --; Exp. 8.5; Determination of Enantiomeric Purity by [superscript 31]P NMR --; Exp. 8.6; Determination of Absolute Configuration by the Advanced Mosher Method --; Exp. 8.7; Aromatic Solvent-Induced Shift (ASIS) --; Exp. 8.8; NMR Spectroscopy of OH Protons and H/D Exchange --; Exp. 8.9; Water Suppression Using an Exchange Reagent --; Exp. 8.10; Isotope Effects on Chemical Shielding --; Exp. 8.11; pK[subscript a] Determination by [superscript 13]C NMR --; Exp. 8.12; Determination of Association Constants K[subscript a] --; Exp. 8.13; Saturation Transfer Difference NMR --; Exp. 8.14; The Relaxation Reagent Cr(acac)[subscript 3] --; Exp. 8.15; Determination of Paramagnetic Susceptibility by NMR --; Exp. 8.16; [superscript 1]H and [superscript 13]C NMR of Paramagnetic Compounds --; Exp. 8.17; The CIDNP Effect --; Exp. 8.18; Quantitative [superscript 1]H NMR Spectroscopy: Determination of the Alcohol Content of Polish Vodka --; Exp. 8.19; Quantitative [superscript 13]C NMR Spectroscopy with Inverse Gated [superscript 1]H-Decoupling --; Exp. 8.20; NMR Using Liquid-Crystal Solvents --; Chapter 9; Heteronuclear NMR Spectroscopy --; Exp. 9.1; [superscript 1]H-Decoupled [superscript 15]N NMR Spectra Using DEPT --; Exp. 9.2; [superscript 1]H-Coupled [superscript 15]N NMR Spectra Using DEPT --; Exp. 9.3; [superscript 19]F NMR Spectroscopy --; Exp. 9.4; [superscript 29]Si NMR Spectroscopy Using DEPT --; Exp. 9.5; [superscript 29]Si NMR Spectroscopy Using Spin-Lock Polarization --; Exp. 9.6; [superscript 119]Sn NMR Spectroscopy --; Exp. 9.7; [superscript 2]H NMR Spectroscopy --; Exp. 9.8; [superscript 11]B NMR Spectroscopy --; Exp. 9.9; [superscript 17]O NMR Spectroscopy Using RIDE --; Exp. 9.10; [superscript 47/49]Ti NMR Spectroscopy Using ARING --; Chapter 10; The Second Dimension --; Exp. 10.1; 2D J-Resolved [superscript 1]H NMR Spectroscopy --; Exp. 10.2; 2D J-Resolved [superscript 13]C NMR Spectroscopy --; Exp. 10.3; The Basic H,H-COSY Experiment --; Exp. 10.4; Long-Range COSY --; Exp. 10.5; Phase-Sensitive COSY --; Exp. 10.6; Phase-Sensitive COSY-45 --; Exp. 10.7; E.COSY --; Exp. 10.8; Double-Quantum-Filtered COSY with Presaturation --; Exp. 10.9; Fully Coupled C,H Correlation (FUCOUP) --; Exp. 10.10; C,H-Correlation by Polarization Transfer (HETCOR) --; Exp. 10.11; Long-Range C,H-Correlation by Polarization Transfer --; Exp. 10.12; C,H Correlation via Long-Range Couplings (COLOC) --; Exp. 10.13; The Basic HMQC Experiment --; Exp. 10.14; Phase-Sensitive HMQC with BIRD Filter and GARP Decoupling --; Exp. 10.15; Poor Man's Gradient HMQC --; Exp. 10.16; Phase-Sensitive HMBC with BIRD Filter
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