000 09312cam a22003734a 4500
001 u5273
003 SA-PMU
005 20210418122833.0
008 060807s2004 gw a b 001 0 eng c
010 _a 2006455166
040 _aHUA
_beng
_cHUA
_dDLC
_dERE
_dOHX
_dBAKER
_dVRC
_dUKM
_dMUQ
_dYDXCP
_dBTCTA
_dOCLCG
_dIG#
_dLMR
_dDEBBG
_dOCL
_dNMC
020 _a3527310673
020 _a9783527310678
035 _a(OCoLC)55685718
_z(OCoLC)56647284
042 _apcc
050 0 0 _aQD96.N8
_bB47 2004
082 0 0 _a543/.66
_222
100 1 _aBerger, Stefan,
_d1946-
245 1 0 _a200 and more NMR experiments :
_ba practical course /
_cStefan Berger, Siegmar Braun.
246 3 _aTwo hundred and more NMR experiments
246 3 0 _aNMR experiments
250 _a3rd rev. and expanded ed.
260 _aWeinheim :
_bWiley-VCH,
_cc2004.
300 _axv, 838 p. :
_bill. ;
_c24 cm.
504 _aIncludes bibliographical references and index.
505 0 0 _gChapter 1.
_tThe NMR Spectrometer --
_g1.1.
_tComponents of an NMR Spectrometer --
_g1.1.1.
_tThe Magnet --
_g1.1.2.
_tThe Spectrometer Cabinet --
_g1.1.3.
_tThe Computer --
_g1.1.4.
_tMaintenance --
_g1.2.
_tTuning a Probe-Head --
_g1.3.
_tThe Lock Channel --
_g1.4.
_tThe Art of Shimming --
_g1.4.1.
_tThe Shim Gradients --
_g1.4.2.
_tThe Shimming Procedure --
_g1.4.3.
_tGradient Shimming --
_gChapter 2.
_tDetermination of Pulse-Duration --
_gExp. 2.1.
_tDetermination of the 90[degree] [superscript 1]H Transmitter Pulse-Duration --
_gExp. 2.2.
_tDetermination of the 90[degree] [superscript 13]C Transmitter Pulse-Duration --
_gExp. 2.3.
_tDetermination of the 90[degree] [superscript 1]H Decoupler Pulse-Duration --
_gExp. 2.4.
_tThe 90[degree] [superscript 1]H Pulse with Inverse Spectrometer Configuration --
_gExp. 2.5.
_tThe 90[degree] [superscript 13]C Decoupler Pulse with Inverse Configuration --
_gExp. 2.6.
_tComposite Pulses --
_gExp. 2.7.
_tRadiation Damping --
_gExp. 2.8.
_tPulse and Receiver Phases --
_gExp. 2.9.
_tDetermination of Radiofrequency Power --
_gChapter 3.
_tRoutine NMR Spectroscopy and Standard Tests --
_gExp. 3.1.
_tThe Standard [superscript 1]H NMR Experiment --
_gExp. 3.2.
_tThe Standard [superscript 13]C NMR Experiment --
_gExp. 3.3.
_tThe Application of Window Functions --
_gExp. 3.4.
_tComputer-Aided Spectral Analysis --
_gExp. 3.5.
_tLine Shape Test for [superscript 1]H NMR Spectroscopy --
_gExp. 3.6.
_tResolution Test for [superscript 1]H NMR Spectroscopy --
_gExp. 3.7.
_tSensitivity Test for [superscript 1]H NMR Spectroscopy --
_gExp. 3.8.
_tLine Shape Test for [superscript 13]C NMR Spectroscopy --
_gExp. 3.9.
_tASTM Sensitivity Test for [superscript 13]C NMR Spectroscopy --
_gExp. 3.10.
_tSensitivity Test for [superscript 13]C NMR Spectroscopy --
_gExp. 3.11.
_tQuadrature Image Test --
_gExp. 3.12.
_tDynamic Range Test for Signal Amplitudes --
_gExp. 3.13.
_t13[degree] Phase Stability Test --
_gExp. 3.14.
_tRadiofrequency Field Homogeneity --
_gChapter 4.
_tDecoupling Techniques --
_gExp. 4.1.
_tDecoupler Calibration for Homonuclear Decoupling --
_gExp. 4.2.
_tDecoupler Calibration for Heteronuclear Decoupling --
_gExp. 4.3.
_tLow-Power Calibration for Heteronuclear Decoupling --
_gExp. 4.4.
_tHomonuclear Decoupling --
_gExp. 4.5.
_tHomonuclear Decoupling at Two Frequencies --
_gExp. 4.6.
_tThe Homonuclear SPT Experiment --
_gExp. 4.7.
_tThe Heteronuclear SPT Experiment --
_gExp. 4.8.
_tThe Basic Homonuclear NOE Difference Experiment --
_gExp. 4.9.
_t1D Nuclear Overhauser Difference Spectroscopy --
_gExp. 4.10.
_t1D NOE Spectroscopy with Multiple Selective Irradiation --
_gExp. 4.11.
_t[superscript 1]H Off-Resonance Decoupled [superscript 13]C NMR Spectra --
_gExp. 4.12.
_tThe Gated [superscript 1]H-Decoupling Technique --
_gExp. 4.13.
_tThe Inverse Gated [superscript 1]H-Decoupling Technique --
_gExp. 4.14.
_t[superscript 1]H Single-Frequency Decoupling of [superscript 13]C NMR Spectra --
_gExp. 4.15.
_t[superscript 1]H Low-Power Decoupling of [superscript 13]C NMR Spectra --
_gExp. 4.16.
_tMeasurement of the Heteronuclear Overhauser Effect --
_gChapter 5.
_tDynamic NMR Spectroscopy --
_gExp. 5.1.
_tLow-Temperature Calibration Using Methanol --
_gExp. 5.2.
_tHigh-Temperature Calibration Using 1,2-Ethanediol --
_gExp. 5.3.
_tDynamic [superscript 1]H NMR Spectroscopy on Dimethylformamide --
_gExp. 5.4.
_tThe Saturation Transfer Experiment --
_gExp. 5.5.
_tMeasurement of the Rotating-Frame Relaxation Time T[subscript 1 rho] --
_gChapter 6.
_t1D Multipulse Sequences --
_gExp. 6.1.
_tMeasurement of the Spin-Lattice Relaxation Time T[subscript 1] --
_gExp. 6.2.
_tMeasurement of the Spin-Spin Relaxation Time T[subscript 2] --
_gExp. 6.3.
_t[superscript 13]C NMR Spectra with SEFT --
_gExp. 6.4.
_t[superscript 13]C NMR Spectra with APT --
_gExp. 6.5.
_tThe Basic INEPT Technique --
_gExp. 6.6.
_tINEPT+ --
_gExp. 6.7.
_tRefocused INEPT --
_gExp. 6.8.
_tReverse INEPT --
_gExp. 6.9.
_tDEPT-135 --
_gExp. 6.10.
_tEditing [superscript 13]C NMR Spectra Using DEPT --
_gExp. 6.11.
_tDEPTQ --
_gExp. 6.12.
_tMultiplicity Determination Using PENDANT --
_gExp. 6.13.
_t1D-INADEQUATE --
_gExp. 6.14.
_tThe BIRD Filter --
_gExp. 6.15.
_tTANGO --
_gExp. 6.16.
_tThe Heteronuclear Double-Quantum Filter --
_gExp. 6.17.
_tPurging with a Spin-Lock Pulse --
_gExp. 6.18.
_tWater Suppression by Presaturation --
_gExp. 6.19.
_tWater Suppression by the Jump-and-Return Method --
_gChapter 7.
_tNMR Spectroscopy with Selective Pulses --
_gExp. 7.1.
_tDetermination of a Shaped 90[degree] [superscript 1]H Transmitter Pulse --
_gExp. 7.2.
_tDetermination of a Shaped 90[degree] [superscript 1]H Decoupler Pulse --
_gExp. 7.3.
_tDetermination of a Shaped 90[degree] [superscript 13]C Decoupler Pulse --
_gExp. 7.4.
_tSelective Excitation Using DANTE --
_gExp. 7.5.
_tSELCOSY --
_gExp. 7.6.
_tSELINCOR: Selective Inverse H,C Correlation via [superscript 1]J(C,H) --
_gExp. 7.7.
_tSELINQUATE --
_gExp. 7.8.
_tSelective TOCSY --
_gExp. 7.9.
_tINAPT --
_gExp. 7.10.
_tDetermination of Long-Range C,H Coupling Constants --
_gExp. 7.11.
_tSELRESOLV --
_gExp. 7.12.
_tSERF --
_gChapter 8.
_tAuxiliary Reagents, Quantitative Determinations, and Reaction Mechanisms --
_gExp. 8.1.
_tSignal Separation Using a Lanthanide Shift Reagent --
_gExp. 8.2.
_tSignal Separation of Enantiomers Using a Chiral Shift Reagent --
_gExp. 8.3.
_tSignal Separation of Enantiomers Using a Chiral Solvating Agent --
_gExp. 8.4.
_tDetermination of Enantiomeric Purity with Pirkle's Reagent --
_gExp. 8.5.
_tDetermination of Enantiomeric Purity by [superscript 31]P NMR --
_gExp. 8.6.
_tDetermination of Absolute Configuration by the Advanced Mosher Method --
_gExp. 8.7.
_tAromatic Solvent-Induced Shift (ASIS) --
_gExp. 8.8.
_tNMR Spectroscopy of OH Protons and H/D Exchange --
_gExp. 8.9.
_tWater Suppression Using an Exchange Reagent --
_gExp. 8.10.
_tIsotope Effects on Chemical Shielding --
_gExp. 8.11.
_tpK[subscript a] Determination by [superscript 13]C NMR --
_gExp. 8.12.
_tDetermination of Association Constants K[subscript a] --
_gExp. 8.13.
_tSaturation Transfer Difference NMR --
_gExp. 8.14.
_tThe Relaxation Reagent Cr(acac)[subscript 3] --
_gExp. 8.15.
_tDetermination of Paramagnetic Susceptibility by NMR --
_gExp. 8.16.
_t[superscript 1]H and [superscript 13]C NMR of Paramagnetic Compounds --
_gExp. 8.17.
_tThe CIDNP Effect --
_gExp. 8.18.
_tQuantitative [superscript 1]H NMR Spectroscopy: Determination of the Alcohol Content of Polish Vodka --
_gExp. 8.19.
_tQuantitative [superscript 13]C NMR Spectroscopy with Inverse Gated [superscript 1]H-Decoupling --
_gExp. 8.20.
_tNMR Using Liquid-Crystal Solvents --
_gChapter 9.
_tHeteronuclear NMR Spectroscopy --
_gExp. 9.1.
_t[superscript 1]H-Decoupled [superscript 15]N NMR Spectra Using DEPT --
_gExp. 9.2.
_t[superscript 1]H-Coupled [superscript 15]N NMR Spectra Using DEPT --
_gExp. 9.3.
_t[superscript 19]F NMR Spectroscopy --
_gExp. 9.4.
_t[superscript 29]Si NMR Spectroscopy Using DEPT --
_gExp. 9.5.
_t[superscript 29]Si NMR Spectroscopy Using Spin-Lock Polarization --
_gExp. 9.6.
_t[superscript 119]Sn NMR Spectroscopy --
_gExp. 9.7.
_t[superscript 2]H NMR Spectroscopy --
_gExp. 9.8.
_t[superscript 11]B NMR Spectroscopy --
_gExp. 9.9.
_t[superscript 17]O NMR Spectroscopy Using RIDE --
_gExp. 9.10.
_t[superscript 47/49]Ti NMR Spectroscopy Using ARING --
_gChapter 10.
_tThe Second Dimension --
_gExp. 10.1.
_t2D J-Resolved [superscript 1]H NMR Spectroscopy --
_gExp. 10.2.
_t2D J-Resolved [superscript 13]C NMR Spectroscopy --
_gExp. 10.3.
_tThe Basic H,H-COSY Experiment --
_gExp. 10.4.
_tLong-Range COSY --
_gExp. 10.5.
_tPhase-Sensitive COSY --
_gExp. 10.6.
_tPhase-Sensitive COSY-45 --
_gExp. 10.7.
_tE.COSY --
_gExp. 10.8.
_tDouble-Quantum-Filtered COSY with Presaturation --
_gExp. 10.9.
_tFully Coupled C,H Correlation (FUCOUP) --
_gExp. 10.10.
_tC,H-Correlation by Polarization Transfer (HETCOR) --
_gExp. 10.11.
_tLong-Range C,H-Correlation by Polarization Transfer --
_gExp. 10.12.
_tC,H Correlation via Long-Range Couplings (COLOC) --
_gExp. 10.13.
_tThe Basic HMQC Experiment --
_gExp. 10.14.
_tPhase-Sensitive HMQC with BIRD Filter and GARP Decoupling --
_gExp. 10.15.
_tPoor Man's Gradient HMQC --
_gExp. 10.16.
_tPhase-Sensitive HMBC with BIRD Filter
650 0 _aNuclear magnetic resonance spectroscopy.
700 1 _aBraun, Siegmar.
856 4 2 _3Publisher description
_uhttp://catdir.loc.gov/catdir/enhancements/fy0653/2006455166-d.html
856 4 1 _3Table of contents only
_uhttp://catdir.loc.gov/catdir/enhancements/fy0653/2006455166-t.html
942 _cBOOK
994 _aZ0
_bSUPMU
596 _a1
999 _c59
_d59